| 海洋资源的化学——Ⅵ杀螟丹中间体硫氰化物的合成研究 |
| 邢存章[1] 孙玉善[2] 孙明昆[2] |
| 关键词:Ⅵ杀螟丹 中间体 硫氰化物 海洋有机化学 人工合成 |
| 主要内容:This paper deals with the synthesis of 1,3-dithiocyanato-2-dimethylaminopropane by the reaction of 2, 3-dichloro-1-dimethylaminopropane with sodium thiocyanate in H2O,in polar organic solvents CH3OH and 95% CH3CH2OH, and in the presence of several phase transfer catalysts including quaternary ammomium salts and amines. These methods have given a respective yield of 58.4% ,69.5% ,74.1% and 80%, |
| 《山东海洋学院学报》 1985,15(1).-19-30 |
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